Bromobenzene : Organic Synthesis

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Hello friends, In this video we will Synthesise bromobenzene by the direct bromination of benzene in the presence of halogen carrier pyridine
It's a pretty straight forward video and mistakes can kill you very easily.

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Been looking for more good chemistry channels, subscribed!

ScienceWithJames
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p-dibromobenzene can be used to make 6, 6-dibromoindigo, the major constituent of Tyrian purple.

douro
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I would have liked more details on the mechanisms for the reaction taking place.... still liked

YouMockMe
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As soon as I added 100ml of 5% naoh and crude product to sep funnel all the red bromine colour went away and I was left with light yellow transparent emulsion. All instructions up to this point were followed except the quantity of bromine was more like 7-8ml. I continued anyway but this washing step seems to have destroyed my dark product and become an unseperable clear yellow aqueous solution.

Any idea what is wrong?

SodiumInteresting
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Hi, is the pyridine completely recovered at the end of the process? or what happen with this material?

Jose_Osorio
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er, the way you have that set up, with the inverted funnel with very little air space in it, that won't stop a decent suck back, if it ever happened, that is.

ashleyobrien
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Very nice! I never heard that pyridine can be used as catalyst. But how is it possible? You need strong Lewis acid, which can coordinate bromide anions. But Pyridine is Lewis base.

Btw. bromobenzenes have boiling points around 220-225°C, so they don't distill before bromobenzene.

bedlaskybedla
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I did the synthesis too but used FeBr3 :D

foc
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What is chemical type of bromobenzene sir?

mayurnaik
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Bromine in gas phase is so dangerous, its better if do rute via sandmeyer

aribinu
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I just make potassium sulphate but I don't know What sinthezis is next. Can you recommend some easy synthesis?

ЭстХимик
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How could this be converted into chlorobenzene? Would bubbling Cl2 into this solution of bromobenzene convert it? Could a liquid be added?

benjaminpainter
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Hi man is always me.. where you take all of this benzene i really need it

fabri___
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Could iodobenzene be created in a similar way with solid iodine?

KeepAnimeDegenerate
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I love this video! But pls i see that you have a lot of benzene.. you can make prayically everithing! Do some pharmaceticaoul synthesis

fabri___
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Now nitrate the glycerol and cellulose

Prchemist
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